SeekerOfTheForm
Matrice Périnatale
- Inscrit
- 19/10/09
- Messages
- 12
alphasnail a dit:Hey guys. I was wondering if anyone knows a good method of mescaline extraction. I have looked up several very handy ones but none of which mention the possibility of freeze percipitation instead of using the conventional airdry method. I was wondering if freeze precipitation is possible? And if anyone knows the best and easiest method around doing so.
thanks!
Quick and dirty acid-base of whatever you're comfortable with. Some dude I know just makes the tea with a lowered pH from addition of HCl, filters the tea until it's an actual solution (i.e: Clear and colored, not foggy), and adds a bit of NaOH and filters that through a cotton ball. Dilute HCl is then poured through, carrying the resalted alkaloids across the ball and into a seperate dish. This is allowed to evaporate, or heated gently 'til dry and leaves behind anything from (really fucked it up) brown tar, to a tan powder.
At this point, you heat MEK (using a double boiler) and add in the crude extract. Water is added drop by drop to the solution after boiling to dissolve the remnants. Freeze, wait a few days, filter. If it's not up to your standards of purity... do it again. If you have trouble with MEK residue being left behind in the product, a simple acetone wash should get rid of it.
Needless to say, don't attempt to double-boil MEK over a flame or anything stupid like that.